Reagents
and conditions:
(a)
ethyl vinyl ether, AcOH, 25 °C → 100 °C; (b) N-bromosuccinimide (NBS), conc. H2SO4, 25 °C; (c) NHMe2, H2O, 80 °C;
(d) 1,2,3-triazole, K2CO3, DMF, 100 °C;
(e) tetrabutylammonium fluoride (TBAF), tetrahydrofuran (THF),
70 °C; (f) TREAT HF, 130 °C.