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. 2022 Oct 18;13:6158. doi: 10.1038/s41467-022-33927-0

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© The Author(s) 2022

Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.

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Fig. 3 — HADDF-STEM images of the as-synthesized CD-LNMO powder (a), and FFT-filtered images of the I (b), and II (c) regions. d, e HADDF-STEM images of the fully charged CD-LNMO powder. e FFT-filtered images of the marked region in d. f, g Enlarged HADDF-STEM images and corresponding signal profiles of the regions marked with blue and orange boxes in b and e, respectively. The occupancies of TM ions in the 16d and 16c sites are represented by gray and green triangles, respectively. Scale bars in a, d and b, c, e represent 2 and 1 nm, respectively.