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. 2022 Oct 19;12:17459. doi: 10.1038/s41598-022-19951-6

Table 2.

Amount of raw materials used in the synthesis of cPNIPAAM in SC-CO2 and co-solvent of DMF.

Materials Mol Mass (gr)
Difunctionalized polymera 0.000072 0.3
Coupling agent 0.00176 0.45
Activator 0.00356 0.36
SC-CO2 0.86 37.84
DMF 0.0387 2.832 (3 ml)

aDifunctionalized polymer was synthesized in condition of P = 23 MPa during 12 h, T = 70 C, Wi/Wm = 1.5%, Wt/Wi = 83.3%, Mw = 4165 (gr/mol), Mn = 1488 (gr/mol) PDI = 2.8, and Mp = 1039 (gr/mol).