Table 2.
Amount of raw materials used in the synthesis of cPNIPAAM in SC-CO2 and co-solvent of DMF.
| Materials | Mol | Mass (gr) |
|---|---|---|
| Difunctionalized polymera | 0.000072 | 0.3 |
| Coupling agent | 0.00176 | 0.45 |
| Activator | 0.00356 | 0.36 |
| SC-CO2 | 0.86 | 37.84 |
| DMF | 0.0387 | 2.832 (3 ml) |
aDifunctionalized polymer was synthesized in condition of P = 23 MPa during 12 h, T = 70 , Wi/Wm = 1.5%, Wt/Wi = 83.3%, Mw = 4165 (gr/mol), Mn = 1488 (gr/mol) PDI = 2.8, and Mp = 1039 (gr/mol).