Evolution of Rf(N) and Rr(N) during 8 thermomechanical tensile tests in controlled stress between −50 and 80 °C for the printed objects. Equations to calculate Rf(N), and Rr(N) are reported in ESIa.
| Cycle (N) | R f(N)(a) (%) | R r(N)(a) (%) | R f(N)(b) (%) | R r(N)(b) (%) |
|---|---|---|---|---|
| N = 1 | 95.5 | — | 95.5 | — |
| N = 2 | 95.6 | 99.8 | 95.1 | 100.2 |
| N = 3 | 95.5 | 99.8 | 95.2 | 100.0 |
| N = 4 | 95.5 | 99.7 | 95.2 | 99.6 |
| N = 5 | 95.6 | 99.7 | 95.2 | 100.4 |
| N = 6 | 95.3 | 99.8 | 95.2 | 99.8 |
| N = 7 | 96.0 | 100.0 | 95.3 | 100.0 |
| N = 8 | 95.9 | 99.8 | 95.2 | 99.8 |
3D printed samples (30 × 5 × 0.3 mm) were irradiated at 385 nm with an irradiance of 9.8 mW cm−2, postcured 2 minutes at 70 mW cm−2 and evaluated after the post cure (sample noted (a) AZ1 + hν + PChν) and after AZ2 (sample noted (b) AZ1 + hν + PChν + AZ2).