Table 1.
Extract | Rt (min.) | Compounds | % of Total | MW | Formula |
---|---|---|---|---|---|
DCM extract | 6.305 | 2,2,6-trimethyloctane | 3.63 | 156.31 | C11H24 |
6.559 | 2,2,3,5-tetramethylheptane | 0.85 | 156.31 | C11H24 | |
6.886 | 2,3,3-trimethyloctane | 0.62 | 156.31 | C11H24 | |
6.928 | 3,3,5-trimethylheptane | 0.49 | 142.28 | C10H22 | |
7.043 | benzeneacetic acid, 3-tetradecyl ester | 0.24 | 332.50 | C22H36O2 | |
7.431 | 2,2,4,6,6-pentamethylheptane | 6.87 | 170.33 | C12H26 | |
7.659 | 2,3,6,7-tetramethyloctane | 4.55 | 170.33 | C12H26 | |
7.706 | 2,5,9-trimethyldecane | 1.07 | 184.37 | C13H28 | |
7.798 | 5,6-dimethyldecane | 0.21 | 170.33 | C12H26 | |
7.997 | 5-ethyl-2,2,3-trimethylheptane | 7.11 | 170.33 | C12H26 | |
8.034 | 2,6,7-trimethyldecane | 0.73 | 184.37 | C13H28 | |
8.324 | 5-nonanone | 60.01 | 142.24 | C9H18O | |
8.377 | decane | 2.72 | 142.28 | C10H22 | |
8.417 | 4-ethyl-2,2-dimethylhexane | 2.19 | 142.28 | C10H22 | |
8.545 | 3,7-dimethyldecane | 0.97 | 170.33 | C12H26 | |
8.626 | 2,2,4-trimethyl-5-hexen-3-ol | 0.71 | 142.24 | C9H18O | |
8.691 | 2,4-dimethylundecane | 0.47 | 184.37 | C13H28 | |
21.688 | 1,2,3,5,6,7-hexahydro-1,1,4,8-tetramethyl-s-indacene | 5.59 | 214.35 | C16H22 | |
25.641 | 9,9a-bis(acetyloxy)-1,1a,1b,4,4a,7a,7b,8,9,9a-decahydro-4a,7b-dihydroxy-1,1,6,8-tetramethyl-3-[(triphenylmethoxy)methyl]-, [1aR-(1aa,1bß,4aß,7aa,7ba,8a,9ß,9aa)]-5H-cyclopropa[3,4]benz[1,2-e]azulen-5-one | 0.97 | 690.83 | C43H46O8 | |
Total | 100.00 | ||||
Ace extract | 3.231 | triethyl borate | 12.24 | 145.99 | C6H15BO3 |
17.205 | benzoic acid, 2,4-dihydroxy-3,6-dimethylmethyl ester methyl ester | 46.50 | 196.20 | C10H12O4 | |
17.504 | atranorin | 4.34 | 374.35 374.35 374.35 |
C19H18O8 | |
18.952 | 2-heptadecanone | 1.63 | 254.45 | C17H34O | |
19.174 | hexadecanoic acid, methyl ester | 0.54 | 270.45 | C17H34O2 | |
22.757 | E,E,Z-1,3,12-nonadecatriene-5,14-diol | 3.43 | 294.47 | C19H34O2 | |
23.057 | 12-methyl-E,E-2,13-octadecadien-1-ol | 2.75 | 280.49 | C19H36O | |
24.900 | spiculesporic acid | 27.17 | 328.40 | C17H28O6 | |
25.039 | ethyl iso-allocholate | 1.40 | 436.62 | C26H44O5 | |
Total | 100.00 | ||||
MeOH extract | 8.340 | acetophenone | 23.25 | 120.15 | C8H8O |
13.419 | (R)-α-methylbenzenemethanol | 0.36 | 122.16 | C8H10O | |
14.854 | 2,3,3-trimethyl-5-phenyl-1-pentene | 17.52 | 188.31 | C14H20 | |
18.797 | 3-phenylbutyrophenone | 22.46 | 224.30 | C16H16O | |
20.132 | 1,3-diphenyl-2-buten-1-one | 36.41 | 222.28 | C16H14O | |
Total | 100.00 | ||||
MeOH-H2O extract | 14.859 | 2,3,3-trimethyl-5-phenyl-1-pentene | 41.56 | 188.31 | C14H20 |
14.923 | (R*,R*)-5-nitro-1-phenyl-1-hexen-3-ol | 2.04 | 221.25 | C12H15NO3 | |
18.842 | 3-phenylbutyrophenone | 43.36 | 224.30 | C16H16O | |
20.219 | 1,3-diphenyl-2-buten-1-one | 9.65 | 222.28 | C16H14O | |
25.617 | 1,4-diol-1,4-diphenyl-2-butene | 3.39 | 240.30 | C16H16O2 | |
Total | 100.00 | ||||
H2O extract | 7.703 | 2-(2-(2-methoxyethoxy)ethoxy)ethyl 2-methylbutanoate | 5.66 | 248.32 | C12H24O5 |
9.653 | 4,5-dihydro-5-thioxo-1,2,4-triazin-3(2H)-one | 17.77 | 129.14 | C3H3N3OS | |
12.722 | 4,4,5,5-tetramethyl-2-phenyl-1,3,2-dioxaborolane | 14.28 | 204.07 | C12H17BO2 | |
13.531 | 4-octadecenal | 2.90 | 266.46 | C18H34O | |
14.003 | 9-oximino-2,7-diethoxyfluorene | 2.59 | 283.33 | C17H17NO3 | |
21.523 | triphenylphosphine | 56.81 | 262.29 | C18H15P | |
Total | 100.00 |