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. 2022 Oct 20;8(10):673. doi: 10.3390/gels8100673

Table 4.

Binding energies, at. % and interpretation of the components of the core levels of interest for the thermally treated samples.

Sample Core Levels BE (eV) at. (%) Interpretation
TiO2−Zn 2.0% TT Ti 2p C1 458.58 0.78 Ti(IV) vol.
C2 459.78 39.04 Ti(IV) surf.
O 1s C1 529.85 48.77 Ti(IV) (vol + surf)
C2 531.22 9.21 Ti(IV) + Zn(II) + cont
Zn 2p C1 1021.85 2.2 Zn(II)
TiO2−Cu 2.0% TT Ti 2p C1 457.29 6.8 Ti(II)
C2 458.56 12.42 Ti(IV) vol.
C3 459.97 18.12 Ti(IV) surf.
O 1s C1 529.43 29.96 Ti(IV) (vol + surf)
C2 531.13 30.19 Cu(I) + cont
Cu 2p C1 930.95 0.32 Cu(0)
C2 931.91 2.19 Cu(I)