Table 1.
Position | 1 | 2 | ||
---|---|---|---|---|
δC Type | δH (J in Hz) | δC Type | δH (J in Hz) | |
1 | 163.2, C | 163.4, C | ||
2 | 109.3, CH | 6.43, d, 8.2 | 109.7, CH | 6.44, d, 8.2 |
3 | 138.9, CH | 7.38, t, 8.2 | 139.0, CH | 7.39, t, 8.2 |
4 | 108.7, CH | 6.52, d, 8.2 | 109.5, CH | 6.55, d, 8.2 |
4a | 160.8, C | 160.3, C | ||
5 | 74.3, CH | 4.69, brs | 74.6, CH | 4.29, m |
6 | 140.5, C | 29.2, CH | 2.34, m | |
7 | 122.3, CH | 5.61, dq, 4.8,1.7 | 32.0, CH2 | 1.57, dt, 14.8, 2.8 |
2.43, m | ||||
8 | 67.9, CH | 4.55, d, 4.8 | 68.6, CH | 4.44, t, 3.6 |
8a | 74.5, C | 85.4, C | ||
9 | 197.2, C | 196.2, C | ||
9a | 108.4, C | 108.6, C | ||
10a | 86.5, C | 76.4, C | ||
11 | 19.2, CH3 | 1.86, d, 1.7 | 18.1, CH3 | 1.32, d, 7.8 |
12 | 64.1, CH2 | Ha 4.12, d, 13.2 | 60.5, CH2 | Ha 3.83, d, 13.5 |
Hb 4.03, d, 13.2 | Hb 4.28, m |