Skip to main content
. 2022 Sep 29;20(10):616. doi: 10.3390/md20100616

Table 1.

1H (400 MHz) and 13C (100 MHz) NMR data of 1 and 2 in CD3OD.

Position 1 2
δC Type δH (J in Hz) δC Type δH (J in Hz)
1 163.2, C 163.4, C
2 109.3, CH 6.43, d, 8.2 109.7, CH 6.44, d, 8.2
3 138.9, CH 7.38, t, 8.2 139.0, CH 7.39, t, 8.2
4 108.7, CH 6.52, d, 8.2 109.5, CH 6.55, d, 8.2
4a 160.8, C 160.3, C
5 74.3, CH 4.69, brs 74.6, CH 4.29, m
6 140.5, C 29.2, CH 2.34, m
7 122.3, CH 5.61, dq, 4.8,1.7 32.0, CH2 1.57, dt, 14.8, 2.8
2.43, m
8 67.9, CH 4.55, d, 4.8 68.6, CH 4.44, t, 3.6
8a 74.5, C 85.4, C
9 197.2, C 196.2, C
9a 108.4, C 108.6, C
10a 86.5, C 76.4, C
11 19.2, CH3 1.86, d, 1.7 18.1, CH3 1.32, d, 7.8
12 64.1, CH2 Ha 4.12, d, 13.2 60.5, CH2 Ha 3.83, d, 13.5
Hb 4.03, d, 13.2 Hb 4.28, m