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. 2022 Sep 30;20(10):620. doi: 10.3390/md20100620

Table 3.

1H (700 MHz) and 13C (175 MHz) NMR data of compound 7 (DMSO-d6, δ in ppm).

Position δC, Type δH, (J in Hz) Position δC, Type δH, (J in Hz)
2 153.1, C 1′ NH 11.06, s
3 142.6, C 2′ 124.2, CH 7.13, s
4 144.5, CH 8.20, s 3′ 108.3, C
5 140.6, C 4′ 126.8, C
6 142.6, CH 8.40, s 5′ 117.3, CH 7.25, d (7.9)
7 29.5, CH2 2.83, t (8.2) 6′ 118.6, CH 6.91, t (7.4)
8 21.8, CH2 1.56, m 7′ 121.2, CH 7.06, t (7.3)
9 13.8, CH3 1.00, t (7.0) 8′ 111.6, CH 7.35, d (8.1)
10 24.5, CH2 2.73, q (7.5) 9′ 136.0, C
11 14.4, CH3 1.13, t (7.5) 10′ 26.5, CH2 3.35, m a
12 24.5, CH2 2.57, q (7.5) 11′ 58.5, CH2 4.78, t (6.5)
13 13.9, CH3 1.01, t (7.5)

a Signal overlapped with H2O.