Table 3.
Position | δC, Type | δH, (J in Hz) | Position | δC, Type | δH, (J in Hz) |
---|---|---|---|---|---|
2 | 153.1, C | 1′ NH | 11.06, s | ||
3 | 142.6, C | 2′ | 124.2, CH | 7.13, s | |
4 | 144.5, CH | 8.20, s | 3′ | 108.3, C | |
5 | 140.6, C | 4′ | 126.8, C | ||
6 | 142.6, CH | 8.40, s | 5′ | 117.3, CH | 7.25, d (7.9) |
7 | 29.5, CH2 | 2.83, t (8.2) | 6′ | 118.6, CH | 6.91, t (7.4) |
8 | 21.8, CH2 | 1.56, m | 7′ | 121.2, CH | 7.06, t (7.3) |
9 | 13.8, CH3 | 1.00, t (7.0) | 8′ | 111.6, CH | 7.35, d (8.1) |
10 | 24.5, CH2 | 2.73, q (7.5) | 9′ | 136.0, C | |
11 | 14.4, CH3 | 1.13, t (7.5) | 10′ | 26.5, CH2 | 3.35, m a |
12 | 24.5, CH2 | 2.57, q (7.5) | 11′ | 58.5, CH2 | 4.78, t (6.5) |
13 | 13.9, CH3 | 1.01, t (7.5) |
a Signal overlapped with H2O.