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. 2022 Sep 21;14(10):2003. doi: 10.3390/pharmaceutics14102003

Table 13.

Overview of identification of diffraction peaks for polymorphs.

# Sample Polymorph Identification Characteristic Peaks (° 2θ) Ref.
1P Ranitidine hydrochloride * Form 1 17, 21.8, 24.9 [74]
Form 2 20.40, 23.7
2P Chlorhexidine dihydrochloride * Form 1 → initial spectrum 13.9, 18.5, 23.7 [140]
Form 2 → few peaks 5.2
Form 3 → many Bragg peaks 14.9, 28.3
3P γ-Sorbitol * A phase → Sharp peaks, increased milling time 16.6, 30.9 [34]
γ phase 11.6, 25.5
4P Rivastigmine Form II 9.5, 11.3, 14.2, 15.5, 19.1, 20 [141]
Form I → Broadeneing of peaks 5.1, 14.7, 16.5, 17.6, 18.6, 20.4, 21.1
5P o-Aminobenzoic acid FI 10.7, 13.7, 14.35, 16.4, 18.6, 23.5, 24.3, 24.9, 26.2, 27.6, 30.5 [54]
FII 11.2, 15.4, 22.2, 26.7
m-Aminobenzoic acid (FIII form) FI 8.6, 17.2, 24.9
FIII 8.3, 16.8, 17.9, 23.7, 23.7, 24.2, 25.9, 26.6, 27.8
p-aminobenzoic acid β-form 17.2, 17.6, 20, 21.9, 25.5, 27.9
α-PABA 17.1, 19.9, 21.8, 25.3, 27.8
6P Dexamethasone * Form A 7.9, 13.5, 16.0, 17.6 [27]
Form B 7.5, 16.8, 18.4
7P Sofosbuvir * Form I 5.3, 7.6, 9.0, 9.8, 10.3 [79]
Form A 6.2, 8.4, 10.5, 12.8,17.4, 17.9, 18.2, 20.3, 21.1
Form B 7.9, 10.3, 12.3, 16.7, 17.1, 19.3, 20, 20.9
Form V 5.6, 6.9, 7.5, 10, 10.8, 13.8, 16.4, 19.7, 25.4
8P Sulindac * Form I 10.8, 17.6 [69]
Form II 9.3, 16.1
9P Γ-sorbitol * Γ-form 11.7, 25.6 [75]
A-Form 16.7, 31.1
12P Sulfamerazine I 12.6, 14.8, 16.3, 17.4, 20.5, 22.7, 23, 24.6, 31.2, 32.7 [166]
II 14.5, 17.0, 19.2, 21.5, 26.6, 27.4, 27.9