Table 13.
Overview of identification of diffraction peaks for polymorphs.
# | Sample | Polymorph Identification | Characteristic Peaks (° 2θ) | Ref. |
---|---|---|---|---|
1P | Ranitidine hydrochloride * | Form 1 | 17, 21.8, 24.9 | [74] |
Form 2 | 20.40, 23.7 | |||
2P | Chlorhexidine dihydrochloride * | Form 1 → initial spectrum | 13.9, 18.5, 23.7 | [140] |
Form 2 → few peaks | 5.2 | |||
Form 3 → many Bragg peaks | 14.9, 28.3 | |||
3P | γ-Sorbitol * | A phase → Sharp peaks, increased milling time | 16.6, 30.9 | [34] |
γ phase | 11.6, 25.5 | |||
4P | Rivastigmine | Form II | 9.5, 11.3, 14.2, 15.5, 19.1, 20 | [141] |
Form I → Broadeneing of peaks | 5.1, 14.7, 16.5, 17.6, 18.6, 20.4, 21.1 | |||
5P | o-Aminobenzoic acid | FI | 10.7, 13.7, 14.35, 16.4, 18.6, 23.5, 24.3, 24.9, 26.2, 27.6, 30.5 | [54] |
FII | 11.2, 15.4, 22.2, 26.7 | |||
m-Aminobenzoic acid (FIII form) | FI | 8.6, 17.2, 24.9 | ||
FIII | 8.3, 16.8, 17.9, 23.7, 23.7, 24.2, 25.9, 26.6, 27.8 | |||
p-aminobenzoic acid | β-form | 17.2, 17.6, 20, 21.9, 25.5, 27.9 | ||
α-PABA | 17.1, 19.9, 21.8, 25.3, 27.8 | |||
6P | Dexamethasone * | Form A | 7.9, 13.5, 16.0, 17.6 | [27] |
Form B | 7.5, 16.8, 18.4 | |||
7P | Sofosbuvir * | Form I | 5.3, 7.6, 9.0, 9.8, 10.3 | [79] |
Form A | 6.2, 8.4, 10.5, 12.8,17.4, 17.9, 18.2, 20.3, 21.1 | |||
Form B | 7.9, 10.3, 12.3, 16.7, 17.1, 19.3, 20, 20.9 | |||
Form V | 5.6, 6.9, 7.5, 10, 10.8, 13.8, 16.4, 19.7, 25.4 | |||
8P | Sulindac * | Form I | 10.8, 17.6 | [69] |
Form II | 9.3, 16.1 | |||
9P | Γ-sorbitol * | Γ-form | 11.7, 25.6 | [75] |
A-Form | 16.7, 31.1 | |||
12P | Sulfamerazine | I | 12.6, 14.8, 16.3, 17.4, 20.5, 22.7, 23, 24.6, 31.2, 32.7 | [166] |
II | 14.5, 17.0, 19.2, 21.5, 26.6, 27.4, 27.9 |