Table 3. Electrochemical Parameters from EIS of API 5L X60 Steel in 1 M H2SO4–CIs at 25 °C.
| CINH | Rs | Rf | Cf | Rct | Y0 | Cdl | RL | L | RpEIS | IEEIS | |||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| CI | ppm/mM | χ2 | Ω cm2 | μF cm–2 | Ω cm2 | μS sn cm–2 | n | μF cm–2 | Ω cm2 | H cm2 | Ω cm2 | % | |
| blank | 0/0 | 0.096 ± 0.004 | 1.57 ± 0.03 | 2.47 ± 0.04 | 0.169 ± 0.035 | 33 ± 3 | 281 ± 30 | 0.87 | 138 ± 10 | 185 ± 20 | 31 ± 4 | 32 ± 3 | - |
| poly[VIMC4][Im] | 25/3.5 × 10–5 | 0.054 ± 0.001 | 1.27 ± 0.03 | 2.24 ± 0.01 | 0.305 ± 0.004 | 80 ± 3 | 234 ± 8 | 0.83 | 106 ± 5 | 440 ± 24 | 232 ± 7 | 71 ± 3 | 55 ± 2 |
| 50/7.1 × 10–5 | 0.078 ± 0.011 | 1.18 ± 0.21 | 2.34 ± 0.06 | 0.274 ± 0.010 | 93 ± 2 | 225 ± 14 | 0.83 | 102 ± 7 | 540 ± 11 | 281 ± 3 | 83 ± 4 | 61 ± 2 | |
| 75/1.1 × 10–4 | 0.070 ± 0.022 | 1.18 ± 0.16 | 2.28 ± 0.16 | 0.296 ± 0.037 | 106 ± 2 | 223 ± 12 | 0.83 | 102 ± 1 | 650 ± 74 | 318 ± 1 | 94 ± 2 | 66 ± 1 | |
| 100/1.4 × 10–4 | 0.071 ± 0.007 | 1.38 ± 0.04 | 2.49 ± 0.02 | 0.246 ± 0.002 | 150 ± 1 | 192 ± 11 | 0.82 | 90 ± 3 | 867 ± 43 | 318 ± 1 | 132 ± 2 | 76 ± 1 | |
| 125/1.8 × 10–4 | 0.081 ± 0.017 | 1.30 ± 0.09 | 2.52 ± 0.12 | 0.242 ± 0.008 | 154 ± 2 | 196 ± 4 | 0.82 | 93 ± 2 | 895 ± 96 | 318 ± 1 | 135 ± 3 | 76 ± 1 | |
| 150/2.1 × 10–4 | 0.102 ± 0.004 | 1.38 ± 0.01 | 2.69 ± 0.04 | 0.222 ± 0.004 | 159 ± 3 | 209 ± 11 | 0.81 | 96 ± 7 | 852 ± 24 | 318 ± 1 | 138 ± 3 | 77 ± 1 | |
| 175/2.5 × 10–4 | 0.132 ± 0.013 | 1.46 ± 0.08 | 2.33 ± 0.14 | 0.252 ± 0.027 | 166 ± 2 | 187 ± 3 | 0.84 | 97 ± 1 | 1396 ± 11 | 318 ± 1 | 152 ± 3 | 79 ± 2 | |
| 200/2.8 × 10–4 | 0.103 ± 0.001 | 2.06 ± 0.01 | 3.37 ± 0.03 | 0.146 ± 0.005 | 186 ± 7 | 186 ± 1 | 0.82 | 88 ± 1 | 968 ± 12 | 318 ± 1 | 161 ± 8 | 80 ± 1 | |
| poly[VIMC2][Br] | 25/4.1 × 10–5 | 0.072 ± 0.038 | 1.43 ± 0.02 | 2.3 ± 0.010 | 0.286 ± 0.011 | 66 ± 3 | 258 ± 9 | 0.85 | 122 ± 3 | 310 ± 59 | 144 ± 35 | 58 ± 4 | 44 ± 4 |
| 50/8.1 × 10–5 | 0.084 ± 0.002 | 1.42 ± 0.00 | 2.26 ± 0.01 | 0.278 ± 0.001 | 77 ± 2 | 247 ± 7 | 0.83 | 112 ± 2 | 365 ± 21 | 224 ± 22 | 68 ± 2 | 53 ± 1 | |
| 75/1.2 × 10–4 | 0.111 ± 0.002 | 1.31 ± 0.04 | 2.18 ± 0.00 | 0.280 ± 0.001 | 86 ± 2 | 231 ± 13 | 0.84 | 109 ± 4 | 433 ± 46 | 260 ± 25 | 75 ± 2 | 57 ± 1 | |
| 100/1.6 × 10–4 | 0.074 ± 0.050 | 1.42 ± 0.16 | 2.48 ± 0.27 | 0.254 ± 0.020 | 127 ± 3 | 210 ± 15 | 0.83 | 104 ± 8 | 780 ± 14 | 318 ± 1 | 113 ± 1 | 72 ± 2 | |
| 125/2.0 × 10–4 | 0.117 ± 0.014 | 1.33 ± 0.01 | 2.29 ± 0.03 | 0.268 ± 0.001 | 144 ± 1 | 213 ± 6 | 0.84 | 108 ± 6 | 884 ± 2 | 318 ± 1 | 127 ± 1 | 75 ± 1 | |
| 150/2.4 × 10–4 | 0.109 ± 0.036 | 2.78 ± 0.58 | 3.72 ± 0.58 | 0.228 ± 0.015 | 159 ± 1 | 193 ± 5 | 0.84 | 102 ± 5 | 1175 ± 82 | 318 ± 1 | 147 ± 1 | 78 ± 1 | |
| 175/2.8 × 10–4 | 0.098 ± 0.006 | 1.34 ± 0.04 | 2.68 ± 0.02 | 0.223 ± 0.003 | 190 ± 1 | 187 ± 1 | 0.81 | 85 ± 2 | 939 ± 14 | 318 ± 1 | 162 ± 1 | 80 ± 1 | |
| 200/3.3 × 10–4 | 0.121 ± 0.010 | 1.49 ± 0.03 | 2.36 ± 0.05 | 0.253 ± 0.032 | 176 ± 3 | 183 ± 8 | 0.84 | 93 ± 5 | 1231 ± 12 | 318 ± 1 | 158 ± 3 | 80 ± 2 | |
| poly[VIMC4][Br] | 25/3.5 × 10–5 | 0.027 ± 0.006 | 1.56 ± 0.19 | 2.42 ± 0.19 | 0.269 ± 0.037 | 74 ± 3 | 239 ± 10 | 0.84 | 113 ± 4 | 401 ± 47 | 207 ± 36 | 66 ± 3 | 52 ± 2 |
| 50/7.0 × 10–5 | 0.070 ± 0.016 | 1.50 ± 0.07 | 2.39 ± 0.09 | 0.269 ± 0.008 | 82 ± 2 | 228 ± 11 | 0.84 | 109 ± 4 | 454 ± 62 | 266 ± 63 | 74 ± 3 | 56 ± 2 | |
| 75/1.0 × 10–4 | 0.064 ± 0.005 | 1.46 ± 0.05 | 2.38 ± 0.05 | 0.269 ± 0.007 | 94 ± 4 | 226 ± 10 | 0.84 | 107 ± 4 | 547 ± 56 | 318 ± 1 | 84 ± 4 | 62 ± 2 | |
| 100/1.4 × 10–4 | 0.082 ± 0.032 | 1.46 ± 0.02 | 2.5 ± 0.08 | 0.235 ± 0.016 | 141 ± 5 | 191 ± 24 | 0.83 | 92 ± 4 | 875 ± 10 | 318 ± 1 | 125 ± 6 | 74 ± 1 | |
| 125/1.7 × 10–4 | 0.132 ± 0.013 | 1.63 ± 0.82 | 2.58 ± 0.83 | 0.173 ± 0.114 | 149 ± 1 | 200 ± 9 | 0.84 | 102 ± 4 | 837 ± 71 | 318 ± 1 | 131 ± 3 | 76 ± 1 | |
| 150/2.1 × 10–4 | 0.110 ± 0.014 | 1.54 ± 0.15 | 2.47 ± 0.14 | 0.242 ± 0.017 | 171 ± 8 | 176 ± 7 | 0.84 | 90 ± 4 | 1083 ± 16 | 318 ± 1 | 151 ± 9 | 79 ± 1 | |
| 175/2.4 × 10–4 | 0.115 ± 0.006 | 1.99 ± 0.92 | 3.03 ± 0.58 | 0.174 ± 0.076 | 196 ± 1 | 162 ± 20 | 0.83 | 81 ± 2 | 1228 ± 14 | 318 ± 1 | 174 ± 2 | 82 ± 2 | |
| 200/2.8 × 10–4 | 0.150 ± 0.029 | 2.08 ± 0.58 | 2.87 ± 0.57 | 0.121 ± 0.032 | 169 ± 10 | 186 ± 12 | 0.84 | 95 ± 5 | 879 ± 38 | 318 ± 1 | 147 ± 8 | 78 ± 1 | |