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. 2022 Oct 19;61(43):17248–17255. doi: 10.1021/acs.inorgchem.2c02835

Scheme 1. Syntheses of 1-Cl, 2-Cl, and 3-Cl as well as Their Hydrogenation to 1-H, 2-H, and 3-H.

Scheme 1

(i) 0.2 equiv of [nBu4N]Cl, CH2Cl2, rt. (ii) Et2O, rt.