Table 5. Lattice parameters from unconstrained refinement without distortion compensation.
| a (Å) | b (Å) | c (Å) | α (°) | β (°) | γ (°) | |
|---|---|---|---|---|---|---|
| DS1 | 11.848 (1) | 11.858 (3) | 11.907 (1) | 90.21 (1) | 90.33 (1) | 89.97 (1) |
| DS2 | 11.842 (1) | 11.881 (2) | 11.888 (2) | 89.77 (2) | 89.75 (1) | 89.75 (1) |
| DS3 | 11.854 (1) | 11.863 (3) | 11.890 (1) | 89.80 (1) | 90.40 (1) | 90.11 (1) |