Table 7. Free unit-cell refinement with distortions obtained from monoclinic unit-cell symmetry constraint induced during simultaneous unit-cell and distortion refinement.
| a (Å) | b (Å) | c (Å) | α (°) | β (°) | γ (°) | |
|---|---|---|---|---|---|---|
| DS1 | 11.917 (1) | 11.913 (3) | 11.903 (1) | 90.00 (1) | 90.02 (1) | 90.00 (1) |
| DS2 | 11.899 (1) | 11.915 (2) | 11.909 (2) | 90.02 (2) | 90.03 (1) | 89.99 (1) |
| DS3 | 11.900 (1) | 11.910 (3) | 11.909 (1) | 90.00 (1) | 90.08 (1) | 90.01 (1) |