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. 2022 Sep 27;9(Pt 6):735–755. doi: 10.1107/S2052252522007904

Table 7. Free unit-cell refinement with distortions obtained from monoclinic unit-cell symmetry constraint induced during simultaneous unit-cell and distortion refinement.

  a (Å) b (Å) c (Å) α (°) β (°) γ (°)
DS1 11.917 (1) 11.913 (3) 11.903 (1) 90.00 (1) 90.02 (1) 90.00 (1)
DS2 11.899 (1) 11.915 (2) 11.909 (2) 90.02 (2) 90.03 (1) 89.99 (1)
DS3 11.900 (1) 11.910 (3) 11.909 (1) 90.00 (1) 90.08 (1) 90.01 (1)