| Crystal data |
| Chemical formula |
[Ag2(NO3)2(C19H17P)2] |
|
M
r
|
892.35 |
| Crystal system, space group |
Orthorhombic, P
n
a21
|
| Temperature (K) |
150 |
|
a, b, c (Å) |
18.0126 (3), 10.6251 (2), 19.2397 (3) |
|
V (Å3) |
3682.20 (11) |
|
Z
|
4 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
9.75 |
| Crystal size (mm) |
0.21 × 0.15 × 0.12 |
| |
| Data collection |
| Diffractometer |
XtaLAB Synergy R, DW system, HyPix |
| Absorption correction |
Multi-scan (CrysAlis PRO; Rigaku OD, 2022 ▸) |
|
T
min, T
max
|
0.665, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
53360, 7741, 7352 |
|
R
int
|
0.068 |
| (sin θ/λ)max (Å−1) |
0.638 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.044, 0.120, 1.05 |
| No. of reflections |
7741 |
| No. of parameters |
451 |
| No. of restraints |
1 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
2.51, −0.73 |
| Absolute structure |
Flack x determined using 3276 quotients [(I
+)−(I
−)]/[(I
+)+(I
−)] (Parsons et al., 2013 ▸) |
| Absolute structure parameter |
−0.009 (4) |
