Table S6.
Recoveries and precisions (intra- and inter-day) of the QuEChERS for 12 AnCS.
| Compound | Spiked level (μg mL−1) | R%a | Precision (%RSD)b | |
|---|---|---|---|---|
|
| ||||
| Intra-day (n = 3) | Inter-day (n = 9) | |||
| Cy | 0.5 | 94.6 | 2.34 | 8.81 |
| 1 | 97.9 | 2.28 | 5.62 | |
| 5 | 93.7 | 1.27 | 6.13 | |
| Dp | 0.5 | 104.8 | 3.52 | 11.2 |
| 1 | 103.5 | 2.73 | 10.4 | |
| 5 | 94.2 | 1.39 | 9.26 | |
| Mv | 0.5 | 91.4 | 3.14 | 10.1 |
| 1 | 105.3 | 2.32 | 7.53 | |
| 5 | 109.2 | 1.86 | 6.91 | |
| Pe | 0.5 | 93.2 | 4.24 | 9.82 |
| 1 | 102.9 | 3.52 | 10.9 | |
| 5 | 108.5 | 0.784 | 6.33 | |
| Pl | 0.5 | 88.5 | 2.73 | 11.7 |
| 1 | 98.8 | 1.91 | 9.44 | |
| 5 | 98.3 | 0.942 | 8.17 | |
| Pt | 0.5 | 106.4 | 2.6 | 7.45 |
| 1 | 93.2 | 4.1 | 6.82 | |
| 5 | 103.5 | 3.5 | 5.66 | |
| Cy-3-glu | 0.5 | 96.2 | 4.3 | 10.3 |
| 1 | 97.8 | 0.841 | 7.47 | |
| 5 | 105.3 | 0.623 | 5.24 | |
| Dp-3-glu | 0.5 | 96.8 | 4.18 | 8.15 |
| 1 | 113.7 | 3.44 | 6.32 | |
| 5 | 102.4 | 2.86 | 6.78 | |
| Mv-3-glu | 0.5 | 90.6 | 3.15 | 6.68 |
| 1 | 105.3 | 3.22 | 7.59 | |
| 5 | 106.7 | 1.27 | 5.86 | |
| Pe-3-glu | 0.5 | 106.5 | 3.39 | 7.91 |
| 1 | 92.4 | 3.48 | 10.4 | |
| 5 | 90.5 | 2.46 | 8.32 | |
| Pl-3-glu | 0.5 | 94.6 | 4.41 | 8.26 |
| 1 | 104.9 | 2.35 | 9.55 | |
| 5 | 108.4 | 3.72 | 5.37 | |
| Pt-3-glu | 0.5 | 98.3 | 3.53 | 7.14 |
| 1 | 106.8 | 2.67 | 7.36 | |
| 5 | 104.2 | 0.912 | 6.82 | |
a
Recoveries.
b
Relative standard deviation of precision values.