Table S7.
Recoveries and precision (intra- and inter-day) of the UAE for 12 AnCS.
Compound | Spiked level (μg mL−1) | R%a | Precision (%RSD)b | |
---|---|---|---|---|
| ||||
Intra-day (n = 3) | Inter-day (n = 9) | |||
Cy | 0.5 | 88.2 | 2.14 | 14.2 |
1 | 104.4 | 2.73 | 8.94 | |
5 | 114.8 | 0.637 | 7.18 | |
Dp | 0.5 | 89.6 | 3.95 | 8.45 |
1 | 105.4 | 1.82 | 9.72 | |
5 | 104.3 | 1.43 | 6.83 | |
Mv | 0.5 | 94.8 | 4.28 | 9.54 |
1 | 98.3 | 4.15 | 10.2 | |
5 | 109.7 | 1.71 | 8.69 | |
Pe | 0.5 | 111.4 | 3.13 | 8.26 |
1 | 96.9 | 4.25 | 12.8 | |
5 | 94.3 | 2.36 | 10.1 | |
Pl | 0.5 | 88.7 | 3.28 | 7.45 |
1 | 95.1 | 3.93 | 8.52 | |
5 | 97.4 | 0.671 | 6.77 | |
Pt | 0.5 | 108.7 | 3.89 | 13.6 |
1 | 109.6 | 3.46 | 9.41 | |
5 | 113.5 | 2.54 | 10.8 | |
Cy-3-glu | 0.5 | 95.6 | 3.22 | 10.1 |
1 | 90.3 | 3.64 | 9.42 | |
5 | 109.5 | 1.13 | 7.48 | |
Dp-3-glu | 0.5 | 110.9 | 4.97 | 8.53 |
1 | 98.1 | 3.42 | 6.94 | |
5 | 92.6 | 2.93 | 5.56 | |
Mv-3-glu | 0.5 | 109.3 | 2.35 | 11.1 |
1 | 117.6 | 2.43 | 7.85 | |
5 | 98.4 | 1.28 | 7.24 | |
Pe-3-glu | 0.5 | 101.9 | 3.42 | 9.33 |
1 | 98.9 | 3.61 | 5.11 | |
5 | 96.3 | 1.76 | 12.5 | |
Pl-3-glu | 0.5 | 94.1 | 2.83 | 9.68 |
1 | 105.8 | 2.72 | 7.29 | |
5 | 82.4 | 4.19 | 4.86 | |
Pt-3-glu | 0.5 | 107.4 | 4.84 | 10.3 |
1 | 92.5 | 3.15 | 7.91 | |
5 | 109.2 | 2.73 | 6.64 |
Recoveries.
Relative standard deviation of precision values.