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. 2022 Nov 7;12(49):31747–31756. doi: 10.1039/d2ra02593k

Retention time (RT), UV and mass spectral characteristics, and tentative identification of putative bioactive compounds in PEO.

Peak no. RT (min) UV [M–H] Main fragments Tentative identification
1 13.35 279 289 245 Catechin
2 16.39 279 577 289 Procyanidin dimer
3 16.65 269 287 269 3,7,3′,4′′-Tetrahydroxyflavanone
4 17.11 270 579 271, 151 Trihydroxyflavanone-o-deoxyhexosyl-O-hexoside
5 18.68 279 577 289 Procyanidin dimer
6 20.64 279 597 289 Catechin-3-O-rutinoside
7 21.52 321 367 173 4-Feruloylquinic acid
8 23.05 269 271 135 7,3′,4′-Trihydroxyflavanone
9 23.71 320 335 173 Shikimic acid hexoside isomer I
10 24.21 321 335 173 Shikimic acid hexoside isomer II
11 24.67 321 371 Caffeoylglucaricacid
12 28.85 229 327 Trihydroxy-octadecadienoicacid
13 29.90 229 329 Trihydroxy-octadecenoicacid
14 34.44 237 573 Cucurbitacin A
15 43.96 229 295 9-/or 13-Hydroxy-9Z,11E-octadecadienoic acid
16 47.53 237 515 Cucurbitacin D
17 48.16 239 555 357 Cucurbitacin E
18 52.82 229 277 Linolenic acid
19 56.28 239 559 Dihydro-cucurbitacin B
20 59.55 237 807 Colocynthoside B
21 60.84 230 281 Oleic acid
22 63.94 239 557 Cucurbitacin B