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(a) Reusability of Pd01 SACs-MOF (5); reaction conditions: 1.96 mmol substrate, 0.1% mol Pd01 SACs-MOF, 4 atm O2, 150 °C, 450 rpm, 15 h; GC yields. (b) Plausible reaction mechanism for Pd in solution. (c) Reaction scope with Pd(OAc)2 (0.3 mol %). Reaction conditions: 1.96 mmol substrate, 0.3% mol Pd(OAc)2, 4 atm O2, 150 °C, 450 rpm, 4 h. GC yields. *15 h. a0.1% mol Pd01 SACs-MOF, 24 h.
