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. 2022 Nov 4;23(21):13536. doi: 10.3390/ijms232113536

Table 2.

Quantification of the benzoxazinoids and verbascoside in the extracts by HPLC–PDA.

No. Compounds EEt EI ED
g of Compound/100 g of Extract 1
1 DIBOA 4.77 ± 0.11 2.18 ± 0.04 <LOQ
2 HBOA 0.78 ± 0.10 0.41 ± 0.04 0.64 ± 0.04
5 β-OH-verbascoside <LOD <LOQ <LOQ
6 β-OH-verbascoside <LOD 0.42 ± 0.05 <LOQ
8 Verbascoside 1.02 ± 0.13 0.61 ± 0.05 0.77 ± 0.05
9 Luteolin di-glucuronide --- <LOQ <LOQ
10 β-EtOH-verbascoside isomer <LOQ --- ---
11 β-EtOH-verbascoside isomer <LOQ --- ---
12 Hispidulin di-glucuronide --- --- <LOQ
13 Verbascoside isomer <LOD <LOQ <LOQ
14 Hispidulin glucuronide <LOQ 0.52 ± 0.02 0.30 ± 0.02

1 Values are the mean ± standard deviation of three replicates; LOD (limit of detection); LOQ (limit of quantification); EEt—ethanol extract; EI—infusion; ED—decoction.