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. 2022 Oct 25;14(21):4505. doi: 10.3390/polym14214505

Table 1.

Comparison of physical–chemical properties for NEs produced with citrus essential oils and different types of emulsifiers.

EO Type Technique Emulsifier Particle Size–
Average (nm)
PDI Storage Time Reference
Orange EO Spontaneous emulsification and ultrasonic emulsification Tween 80 68.3 0.4–0.2 35 days [46]
Phase inversion
Ultrasonic homogenization Tween 80 94.66 0.22 2 weeks [48]
Ultrasonic homogenization Tween 80 94.66 - 2 weeks [38]
Ultrasonic homogenization Tween 80 21.75 0.753 12 weeks [37]
D-limonene High-pressure
homogenization
Soy lecithin 235.9 - 4 weeks [35]
High-pressure
homogenization
Tween 20 + Glycerol monooleate 130.9 - [35]
High-pressure
homogenization
Clear gum 365.7 - 4 weeks [35]
High-pressure
homogenization
Soy lecithin 239 0.18 [36]
High-pressure
homogenization
Pea proteins 184 0.14 [36]
High-pressure
homogenization
Sugar ester 169 0.07 [36]
High-pressure
homogenization
Tween 20 + Glycerol monooleate 228 0.09 [36]
Phase inversion Polyoxyethylene 40 112 [45]
Mandarin EO Ultrasonic homogenization Tween 80 79.14 0.442 2 weeks [38,48]
High-pressure
microfluidization
Tween 80 17 - 8 weeks [40]
Grapefruit EO Ultrasonic homogenization Tween 80 81.05 0.465 2 weeks [38,48]
Lemon EO Ultrasonic homogenization Tween 80 47.40 0.413 2 weeks [38,48]
Ultrasonic homogenization Tween 80 30.2 0.686 1 week [49]
Ultrasonic homogenization Tween 80 181.5 0.114 [39]
Lime EO Phase inversion Tween 80 21 0.444 4 weeks [43]
Bergamot EO High-pressure
homogenization
Glycerol monooleate: Tween 20 (1:1) 138 0.14 8 weeks [14]