Table 2. 13C NMR Data (δC in ppm) for Compounds 1–8 in CDCl3.
| no. | 1 | 2 | 3 | 4 | 5 | 6 | 7 | 8 |
|---|---|---|---|---|---|---|---|---|
| 1 | 144.0, C | 146.6, C | 145.6, C | 143.0, C | 139.7, C | 67.2, C | 142.1, C | 142.6, C |
| 2 | 24.8, CH2 | 124.2, CH | 125.9, CH | 122.4, CH | 122.6, CH | 31.0, CH2 | 123.2, CH | 124.2, CH |
| 3 | 42.0, CH2 | 35.4, CH2 | 134.6, CH | 120.3, CH | 121.8, CH | 120.8, CH | 121.9, CH | 122.9, CH |
| 4 | 135.4, C | 133.3, C | 78.1, C | 138.9, C | 139.6, C | 135.7, C | 139.0, C | 141.3, C |
| 5 | 125.3, CH | 122.8, CH | 40.9, CH2 | 38.3, CH2 | 39.1, CH2 | 39.3, CH2 | 39.7, CH2 | 40.4, CH2 |
| 6 | 25.9, CH2 | 23.7, CH2 | 23.6, CH2 | 25.1, CH2 | 25.5, CH2 | 24.9, CH2 | 27.1, CH2 | 22.1, CH2 |
| 7 | 39.2, CH2 | 39.5, CH2 | 127.0, CH | 127.3, CH | 36.8, CH2 | 126.3, CH | 75.7, CH | 36.9, CH2 |
| 8 | 134.2, C | 134.1, C | 133.0, C | 133.6, C | 61.1, C | 133.6, C | 75.0, C | 75.2, C |
| 9 | 126.1, CH | 126.3, CH | 39.7, CH2 | 37.0, CH2 | 60.1, CH | 38.7, CH2 | 38.6, CH2 | 74.0, CH |
| 10 | 24.4, CH2 | 25.0, CH2 | 24.9, CH2 | 24.5, CH2 | 24.7, CH2 | 24.4, CH2 | 22.4, CH2 | 26.2, CH2 |
| 11 | 38.7, CH2 | 39.2, CH2 | 124.8, CH | 61.4, CH | 36.9, CH2 | 124.2, CH | 34.2, CH2 | 34.9, CH2 |
| 12 | 138.5, C | 135.5, C | 133.7, C | 61.4, CH | 133.8, C | 131.7, C | 134.6, C | 133.8, C |
| 13 | 120.6, CH | 128.0, CH | 37.1, CH | 38.9, CH2 | 126.9, CH | 36.3, CH2 | 126.0, CH | 126.4, CH |
| 14 | 122.1, CH | 77.6, CH | 121.3, CH | 23.1, CH2 | 22.1, CH2 | 62.5, CH | 25.7, CH2 | 26.3, CH2 |
| 15 | 78.4, C | 27.8, CH | 32.3, CH | 78.1, C | 143.5, C | 30.9, CH | 78.5, C | 139.4, C |
| 16 | 26.3, CH3 | 21.8, CH3 | 22.6, CH3 | 25.9, CH3 | 112.3, CH2 | 18.3, CH3 | 26.3, CH3 | 113.3, CH2 |
| 17 | 26.3, CH3 | 21.8, CH3 | 22.7, CH3 | 26.4, CH3 | 21.4, CH3 | 19.2, CH3 | 26.6, CH3 | 21.6, CH3 |
| 18 | 15.7, CH3 | 18.5, CH3 | 21.9, CH3 | 18.3, CH3 | 17.7, CH3 | 15.6, CH3 | 17.2, CH3 | 16.8, CH3 |
| 19 | 15.7, CH3 | 15.1, CH3 | 14.9, CH3 | 15.1, CH3 | 18.5, CH3 | 16.2, CH3 | 24.0, CH3 | 23.4, CH3 |
| 20 | 18.2, CH3 | 16.4, CH3 | 17.5, CH3 | 17.4, CH3 | 15.1, CH3 | 18.2, CH3 | 16.8, CH3 | 15.8, CH3 |
| 21 | 50.4, CH3 | 55.7, CH3 | 50.0, CH3 | 50.5, CH3 | 50.1, CH3 | 170.7, C | ||
| 22 | 170.9, C | 21.4, CH3 | ||||||
| 23 | 21.4, CH3 |