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. Author manuscript; available in PMC: 2023 Nov 1.
Published in final edited form as: J Electroanal Chem (Lausanne). 2022 Oct 3;924:116865. doi: 10.1016/j.jelechem.2022.116865

Table 4.

TGA and reductive desorption data showing surface coverage for Lipoic acid SAMs on NPG and hb-NPG. The data presented is compared with previously reported values.

Method Substrate Surface coverage for LA SAMs (mol cm−2) Reference

Reductive desorption NPG 2.42 × 10−10 [65]
Flat gold surface 3.5 × 10−10 [66]
Flat gold surface 3.00 × 10−10 [50]
NPG 2.09 × 10−10 Present study
hb-NPG 3.42 × 10−10 Present study
Substrate Wt. change (%) Mass loss (μg) Surface coverage LA mol/cm2
TGA analysis NPG 0.05 3.3 ± 0.7 1.3 × 10−9 Present study
hb-NPG 0.1 6.02 ± 0.03 3.8 × 10−9 Present study