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Polysaccharide fingerprinting method validation was performed using a mixture of three polysaccharide standards. Annotated base peak chromatograms of the oligosaccharide profiles of amylopectin (A), arabinoxylan (B), xyloglucan (C), and the mixture (D) are illustrated. Using oligosaccharide fingerprints, all three polysaccharides were successfully identified in the mixture.
