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. 2022 Oct 25;11(11):1468. doi: 10.3390/antibiotics11111468

Table 3.

Gradient elution conditions of the HPLC-DAD analyses for the identification and quantification of polyphenolic compounds.

Time (Min.) Composition A% (Water+Formic Acid 0.1%) Flow (mL/min)
1 97 0.6
5 77 0.6
12 73 0.6
18 57 0.6
25 52 0.6
32 50 0.6
34 50 0.6
37 35 0.6
40 5 0.6
47 5 0.6
48 97 0.6
60 97 0.6