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. 2022 Oct 28;20(11):675. doi: 10.3390/md20110675

Table 4.

Degree of deacetylation percentages (DD %) of chitosan extracted from shrimp waste by chemical methods.

Shell Origin DD (%) Extraction Condition Minutes Reference
Shrimp shell waste 39.10 2% HCl for DM, 4% NaOH for DP, and 40% NaOH for DA, at DT 65 °C [18]
Shrimp shell waste 40.00 2% HCl for DM, 4% NaOH for DP, and 60% NaOH for DA, at DT 65 °C [18]
Shrimp shell waste 41.00 3% HCl for DM, 4% NaOH for DP, and 40% NaOH for DA, at DT 65 °C [18]
Shrimp shell waste 42.00 3% HCl for DM, 4% NaOH for DP, and 60% NaOH for DA, at DT 65 °C [18]
Shrimp shell waste 61.00 4% HCl for DM, 4% NaOH for DP, and 40% NaOH for DA, at DT 65 °C [18]
Shrimp shell waste 70.00 4% HCl for DM, 4% NaOH for DP, and 60% NaOH for DA, at DT 65 °C [18]
Shrimp shell waste 58.00 5% HCl for DM, 4% NaOH for DP, and 40% NaOH for DA, at DT 65 °C [18]
Shrimp shell waste 67.00 5% HCl for DM, 4% NaOH for DP, and 60% NaOH for DA, at DT 65 °C [18]
Penaeus monodon 45.50 (2%, 3%, 4% ) HCl for DM, 4% NaOH for DP, and 30% NaOH for DA, at DT 65 °C [49]
Penaeus monodon 61.24 (2%, 3%, 4% ) HCl for DM, 4% NaOH for DP, and 40% NaOH for DA, at DT 65 °C [49]
Penaeus monodon 79.57 (2%, 3%, 4% ) HCl for DM, 4% NaOH for DP, and 50% NaOH for DA, at DT 65 °C [49]
Penaeus monodon 81.24 (2%, 3%, 4% ) HCl for DM, 4% NaOH for DP, and 60% NaOH for DA, at DT 65 °C [49]
Shrimp shell waste 76.26 6% HCl for DM, 3.5% NaOH for DP, and 50% NaOH for DA, at DT 70 °C [50]
Shrimp shell waste 81.37 6% HCl for DM, 3.5% NaOH for DP, and 50% NaOH for DA, at DT 80 °C [50]
Shrimp shell waste 81.25 6% HCl for DM, 3.5% NaOH for DP, and 50% NaOH for DA, at DT 90 °C [50]
Shrimp shell waste 84.87 6% HCl for DM, 3.5% NaOH for DP, and 50% NaOH for DA, at DT 100 °C [50]
Litopenaeus vannamei 81.00 DM with 2% HCl for shrimp shells with 16 mesh size, then DP under 4% NaOH, and 45% NaOH for DA, at 600 watts in the microwave for 15 min [53]
Litopenaeus vannamei 72.00 DM with 2% HCl for shrimp shells with 32 mesh size, then DP under 4% NaOH, and 45% NaOH for DA, at 600 watts in the microwave for 15 min [53]
Litopenaeus vannamei 78.00 DM with 2% HCl for shrimp shells with 60 mesh size, then DP under 4% NaOH, and 45% NaOH for DA, at 600 watts in the microwave for 15 min [53]
Litopenaeus vannamei 81.00 DM with 2% HCl for shrimp shells with 16 mesh size, then DP with 4% NaOH, and 45% NaOH for DA at 600 watts in the microwave for six pulses of 5 min [53]
Litopenaeus vannamei 92.00 DM with 2% HCl for shrimp shells with 32 mesh size, then DP with 4% NaOH, and 45% NaOH for DA at 600 watts in the microwave for six pulses of 5 min [53]
Litopenaeus vannamei 89.00 DM with 2% HCl for shrimp shells with 60 mesh size, then DP with 4% NaOH, and 45% NaOH for DA at 600 watts in the microwave for six pulses of 5 min [53]
Pink shrimp shells 97.00 3% HCl for DM, 4% NaOH for DP, heating at 2-atmospheric pressure in the autoclave for 1 h and then steeping in 40% NaOH for DA for 4 days [77]
Brown shrimp shells 92.00 3% HCl for DM, 4% NaOH for DP, heating at 2-atmospheric pressure in the autoclave for 1 h and then steeping in 40% NaOH for DA for 4 days [77]
Pink shrimp shells 94.00 3% HCl for DM, 4% NaOH for DP, and 40% NaOH for DA, and then autoclaved at 2-atmospheric pressure for 3 h [77]
Brown shrimp shells 90.00 3% HCl for DM, 4% NaOH for DP, and 40% NaOH for DA, and then autoclaved at 2-atmospheric pressure for 3 h [77]

Where DM, DP, DA, and DT are demineralization, deproteinization, deacetylation, and deacetylation temperature, respectively.