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| temperature (°C) | time (min) | flow of H2 (sccm) | flow of Ar (sccm) | purpose |
|---|---|---|---|---|
| 60 | 60 | 5 | 45 | saturation with H2 |
| 60 | 120 | 0 | 51.2 | purging the lines |
| 60–460 | 80 | 0 | 51.2 | temperature-programmed desorption |
| 460 | 20 | 0 | 51.2 | elimination of any H2 residue in the sample |
