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. 2021 Sep 15;31(12):1667–1671. doi: 10.4014/jmb.2108.08015

Table 1.

NMR data for thiolactomide (1) in DMSO-d6

Position Thiolactomide (1)

δC δH (J in Hz)
1 205.8
2 58.4 4.59 (m)
3 30.6 a 2.07 (m)
b 2.40 (m)
4 27.1 a 3.28 (m)
b 3.39 (m)
5-NH 8.07 (d, 8.3)
6 176.5
7 34.4 2.38 (quint, 7.0)
8 20.0 1.03 (3H, d, 7.0)
9 19.8 1.01 (3H, d, 7.0)

1H and 13C data were recorded at 800 and 200 MHz, respectively.