Table 3. Data collection and processing.
Values in parentheses are for the highest resolution shell.
| Diffraction source | Rigaku FR-X rotating anode |
| Wavelength (Å) | 1.5418 |
| Temperature (K) | 100 |
| Detector | Rigaku R-AXIS VII image plate |
| Crystal-to-detector distance (mm) | 120 |
| Rotation range per image (°) | 0.5 |
| Total rotation range (°) | 135 |
| Exposure time per image (s) | 60 |
| Space group | P41212 |
| a, b, c (Å) | 61.32, 61.32, 208.57 |
| α, β, γ (°) | 90, 90, 90 |
| Mosaicity (°) | 0.229 |
| Resolution range (Å) | 50.00–1.65 (1.75–1.65) |
| Total No. of reflections | 425548 (32429) |
| No. of unique reflections | 47616 (6313) |
| Completeness (%) | 96.8 (81.0) |
| Multiplicity | 8.9 (5.1) |
| 〈I/σ(I)〉 | 23.4 (6.4) |
| CC1/2 | 0.999 (0.956) |
| R meas | 0.063 (0.222) |
| R p.i.m. | 0.024 (0.128) |
| Overall B factor from Wilson plot (Å2) | 21.7 |