3(MBZTH)·4(1,2-F4DIB)	(MBZTH)·(1,3-F4DIB)	(MBZTH)·2(1,3-F4DIB)	2(MBZTH)·(1,4-F4DIB)
Crystal data
Chemical formula	4C6F4I2·3C7H5NS2	C6F4I2·C7H5NS2	4C6F4I2·2C7H5NS2	C6F4I2·2C7H5NS2
M r	2109.16	569.10	1941.92	736.34
Crystal system, space group	Triclinic, P	Triclinic, P	Monoclinic, P21	Monoclinic, P21/n
a, b, c (Å)	7.9410 (8), 14.8483 (15), 24.641 (3)	7.2175 (4), 8.2675 (5), 14.4498 (9)	4.5581 (3), 34.358 (2), 15.6075 (10)	5.5057 (2), 15.6087 (7), 13.5194 (6)
α, β, γ (°)	79.264 (4), 87.104 (4), 82.784 (4)	97.936 (2), 91.297 (2), 109.178 (2)	90, 94.707 (2), 90	90, 94.259 (2), 90
V (Å3)	2830.9 (5)	804.44 (8)	2436.0 (3)	1158.61 (8)
Z	2	2	2	2
μ (mm−1)	4.69	4.20	5.36	3.12
Crystal size (mm)	0.30 × 0.13 × 0.04	0.33 × 0.27 × 0.06	0.18 × 0.12 × 0.04	0.17 × 0.09 × 0.04
Data collection
T min, T max	0.570, 0.746	0.496, 0.746	0.568, 0.746	0.559, 0.746
No. of measured, independent and observed [I > 2σ(I)] reflections	78566, 12466, 11325	27899, 4701, 4391	56285, 12660, 11766	22270, 3402, 2811
R int	0.067	0.036	0.050	0.049
(sin θ/λ)max (Å−1)	0.642	0.706	0.678	0.706
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S	0.067, 0.220, 1.06	0.018, 0.044, 1.09	0.026, 0.046, 1.09	0.027, 0.057, 1.15
No. of reflections	12466	4701	12660	3402
No. of parameters	704	203	622	149
No. of restraints	66	0	2	0
Δρmax, Δρmin (e Å−3)	2.61, −1.48	1.08, −1.11	1.01, −0.71	0.90, −0.79
Absolute structure	–	–	Refined as an inversion twin	–
Absolute structure parameter	–	–	0.454 (15)	–