TABLE 2.
Summary of data collection and refinement statistics
| Data collection | |
|---|---|
| Diffraction source | MX2, LNLS Brazil. |
| Wavelength (Å) | 1.45867 |
| Resolution range (Å) | 46.58–2.00 (2.07–2.00) |
| Space group | P 65 2 2 |
| Cell dimensions (Å) a b c‐ (°) α β γ | 65.6 65.6243.7–90.0 90.0120.0 |
| Total reflections | 152,893 (9871) |
| Unique reflections | 22,065 (2142) |
| Multiplicity | 10.9 (6.2) |
| Completeness (%) | 99.91 (99.86) |
| Mean I/sigma(I) | 13.5 (2.06) |
| R‐merge | 0.145 (1.07) |
| R‐pim | 0.046 (0.352) |
| CC1/2 | 0.998 (0.793) |
| Refinement | |
| R‐work | 0.2075 |
| R‐free | 0.2152 |
| Number of atoms | 1732 |
| Protein | 1,598 |
| B‐factors | |
| Average | 27.22 |
| Macromolecule | 26.08 |
| Solvent | 39.76 |
| Bonds lengths (Å) | 0.007 |
| Bond angles (°) | 1.02 |
| Ramachandran plot | |
| Favored (%) | 98.54 |
| Allowed (%) | 1.46 |
| Outliers (%) | 0.00 |
Note: Highest‐resolution shell are shown in parentheses.