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. 2022 Nov 4;78(Pt 6):835–841. doi: 10.1107/S2052520622009660

Table 1. Experimental details.

Crystal data
Chemical formula [Pt2Cl4(NH3)2{μ-HN=C(O)Bu t }2]
M r 766.33
Crystal system, space group Monoclinic, C2/c
Temperature (K) 293
a, b, c (Å) 19.3247 (3), 8.8795 (1), 12.7062 (2)
β (°) 108.332 (1)
V3) 2069.65 (5)
Z 4
Radiation type Mo Kα
μ (mm−1) 14.03
Crystal size (mm) 0.77 × 0.24 × 0.21
 
Data collection
Diffractometer Nonius KappaCCD
Absorption correction Multi-scan (SADABS)
T min, T max 0.03, 0.05
No. of measured, independent and observed [I > 2.0σ(I)] reflections 29306, 6496, 4944
R int 0.027
(sin θ/λ)max−1) 0.910
 
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S 0.022, 0.017, 1.12
No. of reflections 4707
No. of parameters 100
H-atom treatment H-atom parameters constrained
Δρmax, Δρmin (e Å−3) 1.30, −1.30

Computer programs: COLLECT (Nonius, 2001), CrysAlis (Oxford Diffraction, 2002), SIR92 (Altomare et al., 1993), CRYSTALS (Betteridge et al., 2003), CAMERON (Watkin et al., 1996).