Table 1. Reduction Dependence of the Relative Percentage Contribution of Different Functional Groups and the Relative Percentage Elemental Composition Estimated by Full Scan Spectra.
group | pristine | 50 °C | 100 °C | 150 °C | 200 °C | |
---|---|---|---|---|---|---|
elemental composition (%) | C | 75.43 | 75.62 | 76.24 | 83.86 | 89.83 |
O | 24.57 | 24.38 | 23.76 | 16.14 | 10.17 | |
C=C/C–C | 30.05 | 36.43 | 40.72 | 71.53 | 83.16 | |
C1S deconvolution | C–OH | 27.15 | 20.14 | 18.88 | 14.86 | 8.20 |
>C=O | 35.33 | 32.74 | 31.65 | 9.32 | 5.11 | |
–COOH | 10.05 | 8.75 | 8.09 | 4.29 | 3.54 | |
O1S deconvolution | –COOH | 16.53 | 16.72 | 17.72 | 46.25 | 35.45 |
>C=O | 30.38 | 46.39 | ||||
C–OH | 83.47 | 83.28 | 82.28 | 23.36 | 18.16 |