Table 1.
Materials used in the study
| Material | Classification | Composition | Application |
|---|---|---|---|
| Adper Scotchbond Multi-purpose (SBMP; 3 M ESPE, St. Paul, MN, USA) | Three-step total-etch adhesive |
Etchant 35% phosphoric acid Primer HEMA, polyalkenoic acid polymer, water Bond HEMA, Bis-GMA, tertiary amines, photoinitiator |
Acid etch for 15 s, water rinse for 10 s, gently air dry for 5 s Apply primer for 10 s, gently air dry for 5 s Apply bond. Gently air dry Light cure 10 s |
| Clearfil SE Bond (SE; Kuraray, Osaka, Japan) | Two-step self-etch adhesive |
Primer 10-Methcryloyloxydecyl Dihydrogen phosphate (MDP), HEMA, hydrophilic dimethacrylates, photoinitiator, amine, water Bond MDP, Bis-GMA, HEMA, hydrophobic dimethacrylate, colloidal silica, photoinitiator |
Apply primer for 20 s, gently air dry for 5 s Apply bond, Gentle air dry Light cure 10 s |
| Estelite quick (Tokuyama, Tokyo, Japan) | Nano-filled composite resin | Bis-GMA, TEGDMA, silica zirconia fillers, silica-titania fillers, photoinitiators | Resin composite placement through incremental technique with each 2.0 mm increment light-cured |
HEMA (hydroxyethyl)methacrylate, BisGMA bisphenol A glycidylmethacrylate, MDP 10-methacryloyloxydecyl dihydrogen phosphate, TEGDMA triethylene glycol dimethacrylate