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. 2022 Dec 8;22:574. doi: 10.1186/s12903-022-02632-1

Table 1.

Materials used in the study

Material Classification Composition Application
Adper Scotchbond Multi-purpose (SBMP; 3 M ESPE, St. Paul, MN, USA) Three-step total-etch adhesive

Etchant 35% phosphoric acid

Primer HEMA, polyalkenoic acid polymer, water

Bond HEMA, Bis-GMA, tertiary amines, photoinitiator

Acid etch for 15 s, water rinse for 10 s, gently air dry for 5 s

Apply primer for 10 s, gently air dry for 5 s

Apply bond. Gently air dry

Light cure 10 s

Clearfil SE Bond (SE; Kuraray, Osaka, Japan) Two-step self-etch adhesive

Primer 10-Methcryloyloxydecyl Dihydrogen phosphate (MDP), HEMA, hydrophilic dimethacrylates, photoinitiator, amine, water

Bond MDP, Bis-GMA, HEMA, hydrophobic dimethacrylate, colloidal silica, photoinitiator

Apply primer for 20 s, gently air dry for 5 s

Apply bond, Gentle air dry

Light cure 10 s

Estelite quick (Tokuyama, Tokyo, Japan) Nano-filled composite resin Bis-GMA, TEGDMA, silica zirconia fillers, silica-titania fillers, photoinitiators Resin composite placement through incremental technique with each 2.0 mm increment light-cured

HEMA (hydroxyethyl)methacrylate, BisGMA bisphenol A glycidylmethacrylate, MDP 10-methacryloyloxydecyl dihydrogen phosphate, TEGDMA triethylene glycol dimethacrylate