Table 1. Data collection and refinement statistics.
| LARGE1ΔCC | |
|---|---|
| Wavelength | 0.9677 |
| Resolution range | 45.64–2.61 (2.69–2.61) |
| Space group | C 2 |
| Unit cell | 196.53 107.38 100.33 90 120.26 90 |
| Total reflections | 140110 |
| Unique reflections | 52821 |
| Multiplicity | 2.7 |
| Completeness (%) | 96.0 (93.0) |
| Mean I/sigma(I) | 4.5 (0.4) |
| R-meas | 18.1 (322.5) |
| CC1/2 | 98.3 (14.9) |
| Reflections used in refinement | 52411 |
| Reflections used for R-free | 1194 |
| R-work | 0.215 |
| R-free | 0.270 |
| Number of atoms | |
| macromolecules | 9685 |
| ligands | 45 |
| solvent | 44 |
| RMSD (bonds) | 0.008 |
| RMSD (angles) | 1.22 |
| Ramachandran favored (%) | 97.03 |
| Ramachandran allowed (%) | 2.88 |
| Ramachandran outliers (%) | 0.00 |
| Rotamer outliers (%) | 3.15 |
| Clashscore | 11.97 |
| Average B-factor | |
| macromolecules | 83.99 |
| ligands | 110.11 |
| solvent | 63.87 |
Statistics for the highest-resolution shell are shown in parentheses.