Table 3. Physical Data of Synthesized Compounds (17–26).
compound | yield (%) | M.P. (°C) | color | Rf |
---|---|---|---|---|
17 | 74 | 213–215 | brown | 0.3b |
18 | 88 | 238–240 | light yellow | 0.2a |
19 | 89 | 176–178 | yellow | 0.6c |
20 | 76 | 203–205 | off white | 0.4a |
21 | 87 | 227–229 | off white | 0.4d |
22 | 82 | 176–178 | yellow | 0.3e |
23 | 81 | 208–210 | off white | 0.5a |
24 | 79 | 256–258 | light brown | 0.4a |
25 | 87 | 228–230 | dark brown | 0.4a |
26 | 84 | 227–229 | off white | 0.4b |
n-hexane/EtOAc = 1:4.
n-hexane/EtOAc = 3:2.
n-hexane/EtOAc = 3:7.
n-hexane/EtOAc = 7:3.
n-hexane/EtOAc = 4:1.