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. 2022 Dec 6;7(50):47251–47264. doi: 10.1021/acsomega.2c06513

Table 3. Physical Data of Synthesized Compounds (17–26).

compound yield (%) M.P. (°C) color Rf
17 74 213–215 brown 0.3b
18 88 238–240 light yellow 0.2a
19 89 176–178 yellow 0.6c
20 76 203–205 off white 0.4a
21 87 227–229 off white 0.4d
22 82 176–178 yellow 0.3e
23 81 208–210 off white 0.5a
24 79 256–258 light brown 0.4a
25 87 228–230 dark brown 0.4a
26 84 227–229 off white 0.4b
a

n-hexane/EtOAc = 1:4.

b

n-hexane/EtOAc = 3:2.

c

n-hexane/EtOAc = 3:7.

d

n-hexane/EtOAc = 7:3.

e

n-hexane/EtOAc = 4:1.