Table 3.
Entry | Base | Yield (%) |
---|---|---|
1 | - | 15 |
2 | NaOAc | 54 |
3 | Na2CO3 | 25 |
4 | K2CO3 | 25 |
5 | KOH | 92 |
a Reaction conditions: 0.268 mmol of 1a (1 eq), 0.161 mmol of TBAB (0.6 eq), 0.563 mmol (2 eq) of base, and 2% w/w of catalyst in 2.5 mL of water under MW irradiation (T = 100 °C, 30 min).