Table 1.
Structural and physical parameters of investigated MNPs.
Sample | XRD Results | Textural Parameters |
Magnetic Parameters ** | |||||||||
---|---|---|---|---|---|---|---|---|---|---|---|---|
Phases | wt% | 2θ (°) (311) |
FWHM (°) | Lattice Parameter a = b = c (Å) |
Crystallite Size (311) (Å) | Crystallite Size (WH) (Å) | SBET (m2g−1) | Pore Volume (cm3g−1) | Ms [emu/g] |
μ/kB [K/Oe] | Quality Factor | |
AM1 | Fe3O4 | 91.2 | 35.619 | 0.627 | 8.357 | 139 | 117 | 36.0 | 0.318 | 83.23 | 0.73 | 6.52 × 10−4 |
Ag | 8.8 | - | - | - | - | - | ||||||
AM1-S1 | Fe3O4 | 97.7 | 35.601 | 0.647 | 8.349 | 135 | 103 | 258.0 | 0.491 | 58.47 | 1.14 | 8.03 × 10−5 |
Ag | 2.3 | - | - | - | - | - | ||||||
AM1-S2 | Fe3O4 | 93 | 35.480 | 0.590 | 8.352 | 148 | 110 | 328.8 | 0.536 | 73.85 | 0.78 | 6.10 × 10−4 |
Ag | 7 | - | - | - | - | - | ||||||
AM2 | Fe3O4 | 81 | 35.507 | 0.609 | 8.368 | 143 | 126 | 55.7 | 0.290 | 60.57 | 0.947 | 6.80 × 10−4 |
Ag | 19 | - | - | - | - | - | ||||||
AM2-S1 | Fe3O4 | 84 | 35.473 | 0.624 | 8.371 | 140 | 119 | 344.6 | 0.471 | 13.41 | 1.29 | 9.52 × 10−4 |
Ag | 16 | - | - | - | - | - | ||||||
AM2-S2 | Fe3O4 | 92.6 | 35.481 | 0.588 | 8.387 | 148 | 127 | 342.5 | 0.475 | 24.87 | 1.29 | 7.20 × 10−4 |
Ag | 7.4 | - | - | - | - | - | ||||||
Reference (00-019-0629) |
- | - | 35.42 | - | 8.396 | - |
T[K] is temperature, H[Oe] is intensity of the applied field and [Oe] stands for [Gauss] |