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. 2022 Dec 21;2022:5297603. doi: 10.1155/2022/5297603

Table 3.

Summary of intraday and interday precisions and accuracies of four analytes in plasma and tissue samples.

Compounds Matrix Concentration (ng/mL) Intraday (n = 6) Interday (n = 18)
Accuracy RSD (%) Accuracy RSD (%)
Chlorogenic acid Plasma 2 104.02 ± 11.91 11.45 100.64 ± 11.67 11.60
4 97.72 ± 9.23 9.45 96.09 ± 7.08 7.36
100 104.42 ± 6.23 5.97 104.29 ± 10.6 10.16
2400 101.22 ± 3.20 3.16 96.59 ± 8.11 8.40
Heart 2 101.90 ± 12.14 11.92 109.34 ± 11.74 10.74
4 99.35 ± 3.89 3.91 93.67 ± 6.13 6.54
100 96.57 ± 4.81 4.98 94.46 ± 7.80 8.26
2400 109.00 ± 5.90 5.41 102.88 ± 6.85 6.66
Liver 2 101.65 ± 2.82 2.78 100.88 ± 5.38 5.33
4 101.45 ± 2.98 2.93 98.59 ± 6.72 6.82
100 100.30 ± 2.89 2.88 97.78 ± 4.89 5.00
2400 95.07 ± 5.74 6.04 97.11 ± 5.58 5.75
Spleen 2 96.40 ± 7.63 7.92 102.14 ± 8.90 8.71
4 95.40 ± 4.20 4.40 101.28 ± 9.61 9.49
100 102.40 ± 2.00 1.95 111.52 ± 7.00 6.27
2400 94.93 ± 4.81 5.07 108.26 ± 10.41 9.62
Lung 2 101.53 ± 6.40 6.30 101.22 ± 7.45 7.36
4 99.75 ± 6.09 6.10 93.33 ± 11.17 11.97
100 108.33 ± 5.47 5.04 111.33 ± 6.49 5.83
2400 100.60 ± 3.35 3.33 101.63 ± 5.07 4.99
Kidney 2 98.12 ± 5.36 5.47 96.23 ± 5.33 5.54
4 100.13 ± 2.17 2.17 92.09 ± 7.21 7.83
100 99.37 ± 5.20 5.23 96.10 ± 6.36 6.62
2400 104.47 ± 5.79 5.54 99.47 ± 6.06 6.10
Small intestine 2 93.27 ± 4.13 4.43 96.03 ± 7.86 8.19
4 86.48 ± 5.09 5.89 93.40 ± 10.75 11.51
100 89.75 ± 7.96 8.87 96.61 ± 10.06 10.41
2400 92.70 ± 6.63 7.16 93.01 ± 5.27 5.66
Stomach 2 105.87 ± 7.87 7.43 107.84 ± 7.45 6.90
4 93.17 ± 7.02 7.53 98.76 ± 6.44 6.52
100 106.00 ± 3.95 3.73 106.35 ± 4.46 4.19
2400 100.63 ± 4.18 4.15 99.41 ± 4.81 4.84
Brain 2 109.27 ± 6.74 6.17 104.39 ± 9.47 9.07
4 101.00 ± 3.81 3.77 101.29 ± 5.42 5.35
100 106.00 ± 4.94 4.66 106.77 ± 7.16 6.70
2400 101.27 ± 2.25 2.22 105.62 ± 7.04 6.67
Naucleactonin C Plasma 5 95.62 ± 12.10 12.65 98.24 ± 10.30 10.48
8 100.53 ± 11.78 11.71 96.43 ± 12.16 12.61
140 99.95 ± 6.49 6.50 95.76 ± 7.18 7.50
2400 97.05 ± 4.80 4.95 95.50 ± 6.23 6.52
Heart 5 111.27 ± 7.32 6.58 107.46 ± 10.58 9.85
8 99.28 ± 5.48 5.52 101.15 ± 11.46 11.33
140 93.45 ± 4.34 4.65 93.19 ± 5.33 5.72
2400 105.92 ± 9.54 9.01 104.46 ± 6.66 6.38
Liver 5 100.90 ± 5.40 5.36 108.30 ± 7.82 7.22
8 99.47 ± 2.82 2.84 100.52 ± 5.00 4.98
140 88.60 ± 2.60 2.93 93.53 ± 6.33 6.77
2400 102.50 ± 1.52 1.48 101.42 ± 2.46 2.42
Spleen 5 111.00 ± 6.99 6.29 104.42 ± 9.31 8.91
8 98.90 ± 3.55 3.59 100.74 ± 6.77 6.72
140 96.07 ± 3.95 4.11 93.72 ± 5.30 5.66
2400 100.02 ± 3.39 3.39 103.13 ± 5.06 4.91
Lung 5 113.83 ± 4.07 3.58 113.44 ± 5.37 4.73
8 103.28 ± 10.46 10.13 102.03 ± 10.16 9.96
140 104.17 ± 3.76 3.61 103.83 ± 4.05 3.90
2400 107.83 ± 4.07 3.77 107.06 ± 5.02 4.69
Kidney 5 100.70 ± 4.28 4.25 103.81 ± 6.61 6.36
8 98.38 ± 5.31 5.40 99.18 ± 4.36 4.39
140 95.37 ± 4.19 4.39 100.44 ± 7.07 7.04
2400 106.80 ± 9.74 9.12 104.87 ± 6.46 6.16
Small intestine 5 109.98 ± 10.97 9.97 105.41 ± 10.19 9.67
8 99.30 ± 8.94 9.01 100.44 ± 9.18 9.14
140 88.73 ± 8.96 10.10 86.31 ± 7.66 8.88
2400 103.30 ± 6.82 6.60 98.26 ± 7.60 7.73
Stomach 5 109.83 ± 7.05 6.42 102.67 ± 10.09 9.83
8 101.58 ± 2.96 2.92 95.73 ± 8.07 8.43
140 94.88 ± 2.74 2.88 92.09 ± 5.17 5.62
2400 113.17 ± 4.88 4.31 108.96 ± 7.21 6.62
Brain 5 105.75 ± 10.81 10.22 105.82 ± 8.77 8.29
8 104.78 ± 7.46 7.12 100.57 ± 8.11 8.06
140 101.22 ± 4.59 4.53 98.93 ± 5.73 5.80
2400 113.83 ± 3.31 2.91 111.39 ± 5.54 4.98
Khaephuoside A Plasma 5 101.63 ± 9.93 9.77 105.66 ± 10.50 9.94
8 101.02 ± 9.64 9.55 101.78 ± 7.85 7.71
120 112.33 ± 4.76 4.24 106.16 ± 6.11 5.76
1800 104.08 ± 4.39 4.21 102.52 ± 4.41 4.31
Heart 5 113.50 ± 9.18 8.09 103.33 ± 10.92 10.57
8 100.82 ± 6.19 6.14 98.68 ± 7.06 7.16
120 96.73 ± 2.92 3.02 89.72 ± 8.01 8.93
1800 109.12 ± 9.45 8.66 102.43 ± 8.13 7.94
Liver 5 99.97 ± 7.06 7.07 101.51 ± 8.49 8.36
8 104.10 ± 5.07 4.87 101.81 ± 4.02 3.95
120 99.33 ± 0.62 0.62 100.43 ± 4.55 4.53
1800 108.00 ± 6.10 5.65 103.94 ± 5.60 5.39
Spleen 5 98.73 ± 11.21 11.35 103.62 ± 9.47 9.14
8 100.98 ± 6.25 6.19 103.08 ± 6.75 6.55
120 99.35 ± 2.52 2.54 109.89 ± 8.84 8.04
1800 109.00 ± 4.60 4.22 113.06 ± 5.36 4.74
Lung 5 108.17 ± 10.19 9.42 109.93 ± 7.6 6.92
8 109.90 ± 11.25 10.24 106.91 ± 9.95 9.31
120 90.32 ± 6.12 6.78 95.54 ± 6.53 6.83
1800 100.73 ± 2.02 2.00 103.65 ± 6.91 6.66
Kidney 5 106.82 ± 7.91 7.40 109.94 ± 6.29 5.72
8 113.67 ± 2.94 2.59 111.40 ± 6.12 5.49
120 105.30 ± 6.14 5.83 107.78 ± 6.91 6.41
1800 105.02 ± 9.81 9.34 108.84 ± 7.60 6.99
Small intestine 5 106.50 ± 8.53 8.01 104.08 ± 10.11 9.71
8 99.98 ± 9.43 9.13 101.89 ± 11.58 11.36
120 89.90 ± 6.84 7.61 93.74 ± 7.80 8.32
1800 104.45 ± 6.22 5.96 105.44 ± 5.15 4.89
Stomach 5 96.63 ± 9.15 9.47 95.98 ± 10.26 10.69
8 90.92 ± 7.96 8.76 97.66 ± 8.61 8.82
120 104.00 ± 6.13 5.90 103.24 ± 5.31 5.15
1800 109.83 ± 4.83 4.40 110.50 ± 4.54 4.11
Brain 5 108.90 ± 9.74 8.95 107.11 ± 7.94 7.41
8 108.55 ± 9.90 9.12 107.23 ± 8.01 7.47
120 113.17 ± 6.71 5.93 110.13 ± 6.09 5.53
1800 100.50 ± 3.99 3.97 108.44 ± 7.63 7.03
3,4-Dimethoxyphenyl-1-O-β-apiofuroseyl(1 ⟶ 2)-β-D-glucopyranoside Plasma 25 109.00 ± 4.05 3.72 101.34 ± 9.10 8.98
50 105.82 ± 10.95 10.35 102.61 ± 7.89 7.69
350 109.83 ± 5.23 4.76 104.49 ± 8.60 8.23
2400 96.82 ± 2.76 2.85 100.71 ± 7.50 7.45
Heart 25 99.12 ± 5.06 5.10 96.73 ± 8.08 8.35
50 96.45 ± 6.75 7.00 98.20 ± 8.28 8.43
350 89.15 ± 4.83 5.42 90.19 ± 6.82 7.56
2400 99.80 ± 10.89 10.91 99.33 ± 7.66 7.71
Liver 25 105.07 ± 6.62 6.30 103.78 ± 6.39 6.16
50 108.48 ± 7.39 6.82 108.22 ± 7.38 6.82
350 112.15 ± 6.89 6.14 113.99 ± 4.83 4.24
2400 98.28 ± 3.67 3.73 100.28 ± 3.24 3.23
Spleen 25 102.03 ± 10.68 10.47 104.78 ± 8.63 8.23
50 99.90 ± 520 5.21 103.82 ± 7.77 7.48
350 97.70 ± 4.12 4.21 109.12 ± 9.07 8.31
2400 100.65 ± 5.46 5.43 110.22 ± 8.94 8.11
Lung 25 96.17 ± 7.59 7.89 99.80 ± 10.99 11.01
50 106.78 ± 7.08 6.63 107.49 ± 8.16 7.59
350 96.42 ± 4.49 4.66 100.05 ± 5.50 5.49
2400 99.67 ± 6.29 6.31 99.32 ± 5.68 5.72
Kidney 25 97.02 ± 9.75 10.05 96.23 ± 9.38 9.74
50 108.00 ± 5.66 5.24 106.69 ± 7.00 6.56
350 99.63 ± 5.83 5.85 100.46 ± 6.78 6.75
2400 96.50 ± 7.41 7.68 97.74 ± 6.31 6.46
Small intestine 25 98.25 ± 8.92 9.08 97.96 ± 7.73 7.90
50 101.58 ± 6.41 6.31 101.89 ± 7.13 7.00
350 89.58 ± 4.27 4.76 98.17 ± 8.39 8.55
2400 100.18 ± 4.77 4.76 101.32 ± 4.83 4.77
Stomach 25 103.63 ± 5.21 5.02 99.07 ± 9.64 9.73
50 101.90 ± 9.32 9.14 97.96 ± 9.33 9.52
350 114.17 ± 3.19 2.79 109.34 ± 6.14 5.62
2400 100.62 ± 3.42 3.40 99.42 ± 4.66 4.69
Brain 25 106.95 ± 12.13 11.34 99.13 ± 11.26 11.36
50 105.78 ± 7.63 7.22 107.10 ± 7.86 7.34
350 110.00 ± 9.01 8.19 112.56 ± 6.93 6.16
2400 99.42 ± 2.90 2.91 101.13 ± 5.44 5.38