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. Author manuscript; available in PMC: 2024 Jan 2.
Published in final edited form as: Angew Chem Int Ed Engl. 2022 Nov 30;62(1):e202210822. doi: 10.1002/anie.202210822

Table 3.

Diazo compound scope.[a]

graphic file with name nihms-1848133-t0004.jpg
[a]

Conditions: 1 (0.2 mmol), 2 (0.4 mmol), and 3 (0.3 mmol). Isolated yields are reported.

[b]

KHCO3 in place of K2CO3.

[c]

0.3 mmol scale at 60 °C (conventional heating) for 16 h.

[d]

K2CO3 was omitted.

[e]

120 °C (MW), 0.2 M.