TABLE 1.
Optimization conditions in the oxidation of 1-octanol to 1-octanal using CCPSF NPs as nanocatalysts under MW irradiation.
| Entry | mg catalyst | MW power (W) | Irradiation time (min) | Yield |
|---|---|---|---|---|
| 1 | 1 | — | reflux (12 h) | 61 |
| 2 | 1 | 300 | 10 | 72 |
| 3 | 1 | 400 | 5 | 91 |
| 4 | 1 | 500 | 2 | 95 |
| 5 | 2 | 500 | 2 | 95 |
| 6 | 3 | 500 | 5 | 89 |
| 7 | 4 | 500 | 10 | 85 |
| 8 | 5 | 500 | 20 | 71 |
That the bold values indicates the selection of optimal conditions.
The optimal conditions: 1 mg of catalyst (CCPSF NPs) and power of microwave irradiation of 500 W for 2 min were used.