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. 2022 Dec 20;10:1015515. doi: 10.3389/fchem.2022.1015515

TABLE 2.

Green oxidation of primary alcohol derivatives to aldehyde derivatives using CCPSF NPs under MW irradiation.

Primary alcohol (A) Aldehyde (B) Time (min) Yield (%) Found M. P. ( °C ) Reported M. P. ( °C ) (Ghalehbandi et al., 2020)
1 graphic file with name FCHEM_fchem-2022-1015515_wc_tfx1.jpg graphic file with name FCHEM_fchem-2022-1015515_wc_tfx2.jpg 2 91 Liq. Liq.
2 graphic file with name FCHEM_fchem-2022-1015515_wc_tfx3.jpg graphic file with name FCHEM_fchem-2022-1015515_wc_tfx4.jpg 3 92 Liq. Liq.
3 graphic file with name FCHEM_fchem-2022-1015515_wc_tfx5.jpg graphic file with name FCHEM_fchem-2022-1015515_wc_tfx6.jpg 2 90 Liq. Liq.
4 graphic file with name FCHEM_fchem-2022-1015515_wc_tfx7.jpg graphic file with name FCHEM_fchem-2022-1015515_wc_tfx8.jpg 2 91 Liq. Liq.
5 graphic file with name FCHEM_fchem-2022-1015515_wc_tfx9.jpg graphic file with name FCHEM_fchem-2022-1015515_wc_tfx10.jpg 2 91 Liq. Liq.
6 graphic file with name FCHEM_fchem-2022-1015515_wc_tfx11.jpg graphic file with name FCHEM_fchem-2022-1015515_wc_tfx12.jpg 2 95 Liq. Liq.
7 graphic file with name FCHEM_fchem-2022-1015515_wc_tfx13.jpg graphic file with name FCHEM_fchem-2022-1015515_wc_tfx14.jpg 2 100 Liq. Liq.
8 graphic file with name FCHEM_fchem-2022-1015515_wc_tfx15.jpg graphic file with name FCHEM_fchem-2022-1015515_wc_tfx16.jpg 2 100 Liq. Liq.
9 graphic file with name FCHEM_fchem-2022-1015515_wc_tfx17.jpg graphic file with name FCHEM_fchem-2022-1015515_wc_tfx18.jpg 2 93 Liq. Liq.
10 graphic file with name FCHEM_fchem-2022-1015515_wc_tfx19.jpg graphic file with name FCHEM_fchem-2022-1015515_wc_tfx20.jpg 2 98 101–103 104
11 graphic file with name FCHEM_fchem-2022-1015515_wc_tfx21.jpg graphic file with name FCHEM_fchem-2022-1015515_wc_tfx22.jpg 2 97 76–77 77
12 graphic file with name FCHEM_fchem-2022-1015515_wc_tfx23.jpg graphic file with name FCHEM_fchem-2022-1015515_wc_tfx24.jpg 2 100 Liq. Liq.
13 graphic file with name FCHEM_fchem-2022-1015515_wc_tfx25.jpg graphic file with name FCHEM_fchem-2022-1015515_wc_tfx26.jpg 2 100 Liq. Liq.
14 graphic file with name FCHEM_fchem-2022-1015515_wc_tfx27.jpg graphic file with name FCHEM_fchem-2022-1015515_wc_tfx28.jpg 2 96 103–106 104–105
15 graphic file with name FCHEM_fchem-2022-1015515_wc_tfx29.jpg graphic file with name FCHEM_fchem-2022-1015515_wc_tfx30.jpg 2 95 Liq. Liq.
16 graphic file with name FCHEM_fchem-2022-1015515_wc_tfx31.jpg graphic file with name FCHEM_fchem-2022-1015515_wc_tfx32.jpg 3 92 Liq. Liq.

Optimal conditions: 1 mg of CCPSF NPs and power of microwave irradiation 500 (W).