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Reaction conditions: 1a (2.0 eq., 0.2 mmol), 2 (1.0 eq., 0.1 mmol), fac-Ir(ppy)3 (1.0 mol%), TMP (3.0 eq., 0.3 mmol), B2Pin2 (3.0 eq., 0.3 mmol), DCE 1.0 mL, 25 °C, N2, 455 nm, 24 h. Isolated yield is based on 2.
