| Crystal data |
| Chemical formula |
[Ag(NO2)(C21H21P)2] |
|
M
r
|
762.57 |
| Crystal system, space group |
Monoclinic, P21/n
|
| Temperature (K) |
150 |
|
a, b, c (Å) |
10.8253 (1), 33.8752 (2), 11.3921 (1) |
| β (°) |
116.880 (1) |
|
V (Å3) |
3726.22 (6) |
|
Z
|
4 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
5.43 |
| Crystal size (mm) |
0.21 × 0.15 × 0.12 |
| |
| Data collection |
| Diffractometer |
XtaLAB Synergy R, DW system, HyPix |
| Absorption correction |
Multi-scan (CrysAlis PRO; Rigaku OD, 2022 ▸) |
|
T
min, T
max
|
0.524, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
46007, 7335, 7025 |
|
R
int
|
0.037 |
| (sin θ/λ)max (Å−1) |
0.617 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.026, 0.066, 1.03 |
| No. of reflections |
7335 |
| No. of parameters |
439 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.45, −0.55 |
