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. Author manuscript; available in PMC: 2023 Jul 27.
Published in final edited form as: J Am Chem Soc. 2022 Jul 14;144(29):13032–13038. doi: 10.1021/jacs.2c05044

Scheme 4. Isolation and utility of α,α-difluorobenzylsilane.a.

Scheme 4.

a Isolated product yields; see Supporting Information for full synthetic details for each entry. b 53% 19F NMR yield; isolated yield reduced due to coelution with protodesilylated compound 38. c 76% 1H NMR yield; isolated yield reduced due to coelution with protodesilylation side product.