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A) Energy‐minimized structures (DFT:B3LYP/6‐31+G*) of capsularenes 1, 8 and 9 with their inner volumes. B) UV/Vis spectra of model compounds tris‐acetal baskets 4,6 and 7 and capsularenes 1, 8 and 9 in CH2Cl2 at 298 K. C) Emission spectra (λ exc=280 nm) of model compounds, tris‐acetal baskets 4, 6 and 7 and capsularenes 1, 8 and 9 in CH2Cl2. D) Cyclic voltammograms of tris‐acetal basket 4, tris‐acetal basket 6, capsularene 1 and capsularene 8 in DMF containing TBAPF6.
