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. 2022 Oct 18;61(47):e202211732. doi: 10.1002/anie.202211732

Scheme 1.

Scheme 1

Generality of the present Ni‐catalyzed reductive cross‐electrophile‐coupling. Isolated yields after flash chromatography are provided, unless otherwise specified. [a] Isolated as a 9 : 1 mixture of Br/I containing alcohols. [b]19F NMR yield based on internal standard (CF3C6H5). Product 3 t resulted too volatile to be isolated. Bpin: boron pinacolate, Nphth: phthalimide, OTf: trifluoromethanesulfonate; TMS: trimethylsilyl.