Table 1. GC Specifications.
| operating variable | specification |
|---|---|
| column | Agilent J&W HP-5(30 m × 0.32 mm × 0.25 μm) |
| detector | flame ionization detector (FID) |
| injector temperature | 548.2 K |
| oven temperature profile | 323.2–523.2 K at 20 K·min–1 |
| detector temperature | 473.2 K |
| carrier gas | helium |
| gas flow rate | 2 mL·min–1 |
| injection volume | 1 μL |
| retention time repeatability | 0.003 |
| method verification (max RMSD) | 0.005 |
| method verification (statistical uncertainty) | 0.004 |