GC/MS | Agilent technologies gas chromatograph |
---|---|
Column | HP-5MS (30 m × 0.25 mm i.d.; film thickness 0.25 μm) |
Detector | MSD 5975 C |
Carrier gas | Helium (1 mL/min flow rate) |
Temperature range | 40 °C (2 min) followed by 25 °C with a rate of 5 °C/min and lastly 300 °C at 30 °C/min (10 min) |
Scanning range | 45 to 650 amu |