Scheme 5.
Synthesis of a) TCCSia‐Ace‐Dex‐N‐Rd (22), b) TCCSia‐Ace‐Dex‐N219−227‐Rd (23), c) TCCSia‐Ace‐Dex‐Rd (24), and d) PEG‐Ace‐Dex‐N‐Rd (25).
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