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. Author manuscript; available in PMC: 2023 Sep 28.
Published in final edited form as: J Am Chem Soc. 2022 Sep 15;144(38):17680–17691. doi: 10.1021/jacs.2c07726

Scheme 4.

Scheme 4.

Allene Scopea

aReactions were run on a 0.25 mmol scale; values of dr, rr, and E/Z were determined by NMR analysis of the unpurified reaction mixture. *Combined yield of both diastereomers. Average of two runs.